About Course
This Chemical Crystallography course would highlight the concepts and applications of the widely used experimental technique of X-ray crystallography.
They could take the students through the lane of crystallographic symmetry to the structure determination and refinement of crystal structures using x-ray diffraction.
Any experimental organic or inorganic chemist would be benefited from this course.
INTENDED AUDIENCE: Ph.D. students and 2nd-year M.Sc students
Course Content
Chemical Crystallography
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Sources of X-Rays, Crystal Systems and Bravais lattices
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3 Crystallographic Symmetries
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Equivalent Points and 1D Lattices
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5 Five Fold Symmetry and 2D Lattices
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6 2D Space Lattices
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7 Crystallographic Point Groups
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8 Stereographic Projecitons of Point Groups
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9 Understanding of Crystallographic Space Groups
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10 2D Projection of Space Groups
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11 3D Space Groups and Equivalent Points
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12 Obtaining Equivalent points
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15 Miller Indices and Planar Densities
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Tutorial 1
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Identification from Intensity Statistics the Correct Crystal System and Presence of Inversion Center
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Data Reduction- Scale and Temperature Factor
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Data Reduction-Lorentz and Polarization Correction
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Data Reduction-Absorption Correction
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Cambridge Structure Database and its Application
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Disorder Treatment using Olex 2
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Disorders in Crystal Structures
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Structure Solution using Olex 2 (Rigaku Diffractometer)
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Structure Solution using Apex II (Bruker Diffractometer)
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Data Handling (Solution and Refinement) using Various Crystallographic Packages
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Understanding the X-Ray Data
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Single Crystal X-Ray Diffractometer
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Structure Refinement
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Systematic Absence Conditions from Special Structure Factor Expression
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Structure Fcator and Electron Density
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Derivation of Friedel’s Law from Structure Factor by Vector Space Diagram
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Experimental Methods and Theoretical Understanding of X-Ray Diffraction
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Introduction to X-Ray Crystallography
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Diffractometers and Detectors
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Diffractometersn
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Single Crystal X-Ray Diffraction Data Collection
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Tutorial
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Special Method of Crystallisation
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Laue’s and Bragg’s Analysis
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Systematic Absences and Crystallisation Methods
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Bragg’s Law in Reciprocal Lattice and Origin of Systematic Absences
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Origin of Reciprocal Lattice
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Representation of Orthorhombic and Tetragonal Space Groups
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Miller Indices for Crystallographic Directions and Planes
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Tutorial 2
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Ceramic Structures
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Cubic Structues and atomic packing factors
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Tutorial 3
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Theory of X-Ray Diffraction
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Student Ratings & Reviews
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